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Sunday, May 10, 2020 | History

6 edition of High resolution NMR in the solid state found in the catalog.

High resolution NMR in the solid state

fundamentals of CP/MAS

by E. O. Stejskal

  • 106 Want to read
  • 9 Currently reading

Published by Oxford University Press in New York .
Written in English

    Subjects:
  • Solids -- Spectra.,
  • Nuclear magnetic resonance spectroscopy.,
  • Solid state chemistry.

  • Edition Notes

    Includes bibliographical references and index.

    StatementE.O. Stejskal, J.D. Memory.
    ContributionsMemory, Jasper D.
    Classifications
    LC ClassificationsQC176.8.O6 S74 1994
    The Physical Object
    Paginationxii, 189 p. :
    Number of Pages189
    ID Numbers
    Open LibraryOL1082918M
    ISBN 100195073800
    LC Control Number94006547

    One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Annual Reports on NMR Spectroscopy. Explore book series content Latest Total line shape analysis of high-resolution NMR spectra. Dmitry A. Cheshkov, Dmitry O. Sinitsyn / Book chapter Full text access. Chapter Three - Recent advances in chlorine, bromine, and iodine solid-state NMR spectroscopy. Patrick M.J.

      13C high-resolution solid-state NMR for structural elucidation of archaeological woods. Progress in Nuclear Magnetic Resonance Spectroscopy , 55 (3), DOI: /ited by: The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in Price: $

    Modern Methods in Solid-state NMR: A Practitioner’s Guide, Paul Hodgkinson (Ed.) The Royal Society of Chemistry ().. Experimental Approaches of NMR Spectroscopy, Methodology and Application to Life Science and Materials Science The Nuclear Magnetic Resonance Society of . Biological Applications of High Resolution Solid-state NMR Spectroscopy. Applied Spectroscopy Reviews , 20 (2), DOI: /Cited by:


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High resolution NMR in the solid state by E. O. Stejskal Download PDF EPUB FB2

The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution by: Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy.

Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. Covers the dramatic developments in the past decade in the applications of high-resolution NMR to the study of solid materials such as inorganic silicates, aluminosilicates, and in particular, zeolites.

High Resolution NMR in the Solid State Fundamentals of CP/MAS E. Stejskal and J. Memory. This text began as a course for physical chemistry and chemical physics students specializing in CP/MAS NMR who wanted to understand the underlying principles of the experiments they were using in the laboratory, and is aimed at that kind of audience.

It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental level.

Luca, H. Heise, and M. Baldus, High-resolution solid-state NMR: Applied to Polypeptides and membrane proteins, Acc. Chem. Res. 36, – (). CrossRef Google Scholar P.T. Eles and C.A. Michal, A DECODOR NMR study of backbone orientation in Nephila clavipes dragline silk under varying strain and draw rate, Biomacromolecules 5, Author: K.V.R.

Chary, Girjesh Govil. high resolution solid state nmr of silicates and zeolites Download high resolution solid state nmr of silicates and zeolites or read online books in PDF, EPUB, Tuebl, and Mobi Format.

Click Download or Read Online button to get high resolution solid state nmr of silicates and zeolites book now. This site is like a library, Use search box in the. We highlight that sufficient hydration of non-crystallized RNA could provide high-resolution solid-state NMR (SSNMR) spectra, with similar spectral quality to the crystallized RNA.

This leads to a greatly simplified RNA preparation approach by ethanol precipitation for high-resolution SSNMR studies. It will.

Abstract. High-resolution solid state NMR and its application to the characterization of solid state inorganic, organic, or hybrid materials, is undergoing rapid developments on both methodological and hardware points of by: 2. High-resolution solid-state NMR (SSNMR) spectroscopy has many advantages as a tool to characterize solid-phase material that finds applications in polymer chemistry, nanotechnology, materials science, biomolecular structure determination, and others, including the pharmaceutical by: 6.

Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches steady-state energy levels, the rotating vector picture, the density matrix, and the product Format: Hardcover.

High-resolution solid-state NMR has recently been extensively applied to study structure and solid-state reactions of inorganic silicates, aluminosilicates and, in particular, zeolites. In addition, a variety of NMR methods including conventional FT NMR techniques have been successfully used to investigate sorbate-sorbent interactions and the structure of adsorbed molecules.

The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level.

Unfortunately the high resolution achievable in liquidBrand: Springer-Verlag Berlin Heidelberg. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy.

Careful attention is given to developing and interrelating four approaches—steady-state energy levels, the rotating vector picture, the density matrix, and the product Manufacturer: Academic Press.

Manipulation and Dilution Tools for Ruling Abundant Species "NMR is dead" was the slogan heard in the late s at least among physicists, until John S. Waugh and his co-workers initiated a series of new NMR experiments, which employed the coherent modulation of interactions by strongBrand: Springer-Verlag Berlin Heidelberg.

: High Resolution NMR in the Solid State: Fundamentals of CP/MAS () by Stejskal, E. O.; Memory, J. and a great selection of similar New, Used and Collectible Books available now at great Range: $52 - $   It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy.

This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental Edition: 2.

By contrast, solid-state NMR spectra are very broad, as the full effects of anisotropic or orientation-dependent interactions are observed in the spectrum. High-resolution NMR spectra can provide the same type of information that is available from corresponding solution NMR spectra, but a number of special techniques/equipment are.

Included are solid-state and high-resolution NMR studies of the molecular structure and dynamic interactions of lipids, proteins, and nucleic acids. The latest developments in NMR zeugmatographic imaging and in musculoskeletal and cardiovascular magnetic resonance imaging are detailed.

t, "High Resolution Solid State NMR" in "High Magnetic Fields: Applications in Condensed Matter Physics and Spectroscopy", LNP Voleds C. Berthier, L.P. Lévy, G. Martinez, Springer Author: Dominique Massiot. The second part mainly deals with the experimental design of solid-state high-resolution NMR experiments to suppress certain interactions and with wide-line experiments.

Finally the principles of NMR imaging and NMR microscopy are described as an alternative method for investigating solids by by:   High-resolution nuclear magnetic resonance spectroscopy at the scale of single cells is achieved by combining a magnetometer consisting of an ensemble of nitrogen–vacancy centres with a Cited by: Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy.

Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product.